Aye, I should've made the distinction clear between RAID 0 and RAID 1 in my initial post. RAID 1 would make sense for backup purposes.
Bassfisher, to answer your question, yes it is possible. The only issue is when you select RAID in your BIOS, all drives connected to that controller will run in RAID or AHCI mode. So if the hard drive that your OS install is on was using "IDE" mode, it'll break it. If it was running in AHCI to begin with then there's no problem.
Secondly, it is worth noting that most motherboards come with multiple SATA controllers on them. Which means it's possible to set one or more controllers to RAID mode, but put the non-RAID'd hard drives onto a separate controller entirely. This is especially useful if the OS installation was done with the SATA port configured in "IDE" control mode.
Quote:
Originally Posted by bassfisher6522
I did a preliminary run of the extra drives in raid 0 (successfully) but upon reboot my primary drive was no where to be seen.
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I'd need more information to follow you... "no where to be seen" in the BIOS, do you mean? That's typical when using RAID, but it should still show up within the boot menu options regardless.